Boronic acid, B-(2,2-dimethyl-1,3-benzodioxol-5-yl)- synthesis
- Product Name:Boronic acid, B-(2,2-dimethyl-1,3-benzodioxol-5-yl)-
- CAS Number:227306-23-2
- Molecular formula:C9H11BO4
- Molecular Weight:193.99
73790-19-9
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$49.00/100mg
227306-23-2
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Yield:227306-23-2 66%
Reaction Conditions:
Stage #1: 5-bromo-2,2-dimethyl-1,3-benzodioxolewith tert.-butyl lithium in tetrahydrofuran;pentane at -78; for 1 h;Inert atmosphere;
Stage #2: with Trimethyl borate in tetrahydrofuran;pentane at -78 - 20; for 2 h;Inert atmosphere;
References:
Fukuda, Tsutomu;Itoyama, Ryosuke;Minagawa, Terufusa;Iwao, Masatomo [Heterocycles,2014,vol. 88,# 2,p. 1121 - 1133]
14005-14-2
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$90.00/500mg
227306-23-2
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73790-19-9
74 suppliers
$49.00/100mg
121-43-7
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$15.00/25ml
227306-23-2
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120-80-9
525 suppliers
$13.00/25g
227306-23-2
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