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ChemicalBook CAS DataBase List (3Z)-3-(6H-benzo[c][1]benzothiepin-11-ylidene)-N,N-dimethylpropan-1-amine
25627-38-7

(3Z)-3-(6H-benzo[c][1]benzothiepin-11-ylidene)-N,N-dimethylpropan-1-amine synthesis

1synthesis methods
27710-82-3 Synthesis
[3-(Dimethylamino)propyl]triphenylphosphonium bromide hydrobromide

27710-82-3
207 suppliers
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1531-77-7 Synthesis
Dibenzo[b,e]thiepin-11(6H)-one

1531-77-7
158 suppliers
$17.00/5g

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Yield:25627-38-7 49%

Reaction Conditions:

with n-butyllithium in tetrahydrofuran;hexane; for 10 h;Ambient temperature;

References:

Polivka, Zdenek;Licha, Irena;Taufmann, Petr;Svatek, Emil;Holubek, Jiri;Protiva, Miroslav [Collection of Czechoslovak Chemical Communications,1987,vol. 52,# 6,p. 1566 - 1581]