3-(2-Methoxyethoxy)prop-1-yne synthesis
- Product Name:3-(2-Methoxyethoxy)prop-1-yne
- CAS Number:31995-08-1
- Molecular formula:C6H10O2
- Molecular Weight:114.14
109-86-4
566 suppliers
$11.00/25g
106-96-7
343 suppliers
$31.00/25g
31995-08-1
29 suppliers
$114.00/1g
Yield:31995-08-1 79%
Reaction Conditions:
Stage #1: 2-methoxy-ethanolwith sodium hydride in tetrahydrofuran;mineral oil at 0; for 1 h;Inert atmosphere;Williamson synthesis;
Stage #2: propargyl bromide in tetrahydrofuran;mineral oil at 0; for 4 h;Inert atmosphere;Williamson synthesis;
References:
Nanashima, Yutaka;Shibata, Rena;Miyakoshi, Ryo;Yokoyama, Akihiro;Yokozawa, Tsutomu [Journal of Polymer Science, Part A: Polymer Chemistry,2012,vol. 50,# 17,p. 3628 - 3640] Location in patent:experimental part
109-86-4
566 suppliers
$11.00/25g
624-65-7
386 suppliers
$25.00/5mL
31995-08-1
29 suppliers
$114.00/1g