3,3-Dimethyl-1-(3-nitrophenyl)triazene synthesis

2synthesis methods

99-09-2 Synthesis

Yield:20241-06-9 44%

Reaction Conditions:

Stage #1: 3-nitro-anilinewith hydrogenchloride;sodium nitrite at 0 - 10;
Stage #2: dimethyl amine in water;cooling;

References:

Manolov, Ilia;Machulla;Momekov [Pharmazie,2006,vol. 61,# 6,p. 511 - 516]

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