3-(4-Chlorophenyl)-1,2,3-oxadiazole-3-ium-5-olate synthesis
- Product Name:3-(4-Chlorophenyl)-1,2,3-oxadiazole-3-ium-5-olate
- CAS Number:829-31-2
- Molecular formula:
- Molecular Weight:0
106-47-8
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829-31-2
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: SiO2 / 0.08 h / 20 °C / microwave irradiation
1.2: 91 percent / aq. sodium hydroxide / ethanol / 0.17 h / Heating
2.1: 95 percent / silica chloride; wet SiO2; sodium nitrite / CH2Cl2 / 2.3 h / 0 - 5 °C
3.1: 81 percent / 1,3-dibromo-5,5-dimethylhydantoin / CH2Cl2 / 4 h / 0 - 5 °C
References:
Azarifar, Davood;Bosra, Hassan Ghasemnejad;Zolfigol, Mohammad-Ali;Tajbaksh, Mahmood [Heterocycles,2006,vol. 68,# 1,p. 175 - 181]
![2-[(4-chlorophenyl)amino]acetic acid](/CAS/GIF/5465-90-7.gif)
5465-90-7
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829-31-2
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![Acetic acid,2-[(4-chlorophenyl)nitrosoamino]-](/CAS/20180527/GIF/13728-11-5.gif)
13728-11-5
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829-31-2
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2521-89-3
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$41.00/1 g
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