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3-(4-METHOXY-2-METHYLPHENYL)-1-PROPENE synthesis

2synthesis methods
27060-75-9 Synthesis
2-Bromo-5-methoxytoluene

27060-75-9
271 suppliers
$8.00/5g

24850-33-7 Synthesis
Allyltributyltin

24850-33-7
181 suppliers
$12.00/5g

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Yield:16964-10-6 97%

Reaction Conditions:

with tris(dibenzylideneacetone)dipalladium (0);2,8,9-tribenzyl-2,3,8,9-tetraaza-1-phosphabicyclo[3,3,3]undecane;cesium fluoride in tetrahydrofuran at 20; for 14 h;Stille cross-coupling;

References:

Su, Weiping;Urgaonkar, Sameer;McLaughlin, Patrick A.;Verkade, John G. [Journal of the American Chemical Society,2004,vol. 126,# 50,p. 16433 - 16439]

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