3,7-DIMETHYL-1-OCTEN-3-OL synthesis
- Product Name:3,7-DIMETHYL-1-OCTEN-3-OL
- CAS Number:18479-49-7
- Molecular formula:C10H20O
- Molecular Weight:156.27
1604-26-8
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Yield: 96.8%
Reaction Conditions:
with 2,2'-ethane-1,2-diylbissulfanyl-bis-ethanol;hydrogen;Lindlar's catalyst at 30; under 1500.15 Torr; for 8 h;Product distribution / selectivity;Autoclave;
Steps:
c.21
Step cExamples 13 to 30A 150 mL-autoclave (Hastelloy) was charged with 40 g of DMOI with a purity of 99.8% and the amount and catalyst as given in table 4. 4.7 mg of the modifier 2,2' ethylene-dithiodiethanol were added. The mixture was heated to 30° C. and hydrogen was added at 2 bar. After reaction, when no up-take of hydrogen was observed any more, the mixture was cooled to 20° C., the catalyst separated by filtration and the mixture analyzed by gas chromatography.
References:
DSM IP ASSETS B.V. US2012/53353, 2012, A1 Location in patent:Page/Page column 5
110-93-0
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1826-67-1
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$51.29/100ml
928-68-7
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18479-49-7
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928-68-7
93 suppliers
$93.00/5mL
18479-49-7
43 suppliers
inquiry