3'-HYDROXYBIPHENYL-4-CARBOXYLIC ACID METHYL ESTER synthesis
- Product Name:3'-HYDROXYBIPHENYL-4-CARBOXYLIC ACID METHYL ESTER
- CAS Number:579511-01-6
- Molecular formula:C14H12O3
- Molecular Weight:228.24
108-43-0
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619-42-1
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579511-01-6
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Yield:579511-01-6 93%
Reaction Conditions:
Stage #1: 4-methoxycarbonylphenyl bromidewith methanol;tetrahydroxydiboron;XPhos-Pd-G2;potassium acetate;XPhos at 80; for 2 h;Inert atmosphere;Suzuki-Miyaura Coupling;
Stage #2: 3-monochlorophenolwith potassium carbonate in water at 80; for 15 h;Inert atmosphere;Suzuki Coupling;
References:
Molander, Gary A.;Trice, Sarah L. J.;Kennedy, Steven M. [Journal of Organic Chemistry,2012,vol. 77,# 19,p. 8678 - 8688]
140483-59-6
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1107641-09-7
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579511-01-6
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99768-12-4
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579511-01-6
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