3-IODOBENZOYLACETONITRILE synthesis
- Product Name:3-IODOBENZOYLACETONITRILE
- CAS Number:247206-80-0
- Molecular formula:C9H6INO
- Molecular Weight:271.05
Yield:247206-80-0 8.3 g
Reaction Conditions:
Stage #1: acetonitrilewith lithium diisopropyl amide in tetrahydrofuran;hexane;
Stage #2: 3-iodobenzoic acid methyl ester in tetrahydrofuran;hexane at -50; for 3 h;
References:
Goldstein, David M.;Alfredson, Tom;Bertrand, Jay;Browner, Michelle F.;Clifford, Ken;Dalrymple, Stacie A.;Dunn, James;Freire-Moar, Jose;Harris, Seth;Labadie, Sharada S.;La Fargue, JoAnn;Lapierre, Jean Marc;Larrabee, Susan;Li, Fujun;Papp, Eva;McWeeney, Daniel;Ramesha, Chakk;Roberts, Rick;Rotstein, David;San Pablo, Bong;Sjogren, Eric B.;So, On-Yee;Talamas, Francisco X.;Tao, Will;Trejo, Alejandra;Villasenor, Armando;Welch, Mary;Welch, Teresa;Weller, Paul;Whiteley, Phyllis E.;Young, Kelly;Zipfel, Sheila [Journal of Medicinal Chemistry,2006,vol. 49,# 5,p. 1562 - 1575]
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247206-80-0
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