2-chloro-4-(4-chlorophenyl)-6-phenyl-1,3,5-triazine synthesis
- Product Name:2-chloro-4-(4-chlorophenyl)-6-phenyl-1,3,5-triazine
- CAS Number:30894-93-0
- Molecular formula:C15H9Cl2N3
- Molecular Weight:302.16
17513-09-6
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Yield: 80%
Reaction Conditions:
with trichlorophosphate in acetonitrile for 1 h;Reflux;
Steps:
1.3 Step 3) Preparation of Compound A
N'-cyanobenzimidamide(16.8 g, 115 mmol),Compound A-2 (21 g, 115 mmol)And phosphorous oxychloride (12 mL, 128 mmol)Was added to 500 mL of acetonitrile, followed by stirring and refluxing for 1 hour.After cooling to room temperature, the resulting solid was filtered,Washed with water and ethanol, and dried to obtain Compound A (27.6 g, yield 80%)..
References:
LG Chem, Ltd.;Kang Min-yeong;Park Tae-yun;Cho Seong-mi;Moon Jeong-uk;Jeong Min-u;Lee Jeong-ha KR2019/2206, 2019, A Location in patent:Paragraph 0142; 0143; 0150; 0151
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