ETHYL 2-[(5-AMINO-1,3,4-THIADIAZOL-2-YL)THIO]ACETATE synthesis

2synthesis methods

105-36-2 Synthesis

2349-67-9 Synthesis

Yield:32418-24-9 82%

Reaction Conditions:

Stage #1: 2-Amino-5-mercapto-1,3,4-thiadiazolewith potassium hydroxide in ethanol; for 0.166667 h;
Stage #2: ethyl bromoacetate in ethanol; for 2 h;

References:

Gao, Yaojun;Samanta, Sanjay;Cui, Taian;Lam, Yulin [ChemMedChem,2013,vol. 8,# 9,p. 1554 - 1560] Location in patent:supporting information

105-39-5 Synthesis

2349-67-9 Synthesis

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