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ChemicalBook CAS DataBase List 10,10-diphenyl-5,10-dihydrodibenzo[b,e][1,4]azasiline
3508-62-1

10,10-diphenyl-5,10-dihydrodibenzo[b,e][1,4]azasiline synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / toluene
2: sodium hydride / N,N-dimethyl-formamide
3: n-butyllithium / diethyl ether
4: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene; water

References:

Sun, Jin Won;Baek, Jang Yeol;Kim, Kwon-Hyeon;Moon, Chang-Ki;Lee, Jeong-Hwan;Kwon, Soon-Ki;Kim, Yun-Hi;Kim, Jang-Joo [Chemistry of Materials,2015,vol. 27,# 19,p. 6675 - 6681]