ChemicalBook CAS DataBase List 4-(1-ADAMANTYL)PHENOL

4-(1-ADAMANTYL)PHENOL synthesis

12synthesis methods

Product Name:4-(1-ADAMANTYL)PHENOL
CAS Number:29799-07-3
Molecular formula:C16H20O
Molecular Weight:228.33

768-90-1 Synthesis

768-90-1
391 suppliers
$10.00/5g

108-95-2 Synthesis

108-95-2
708 suppliers
$14.00/25g

29799-07-3
132 suppliers
$9.00/250mg

Yield:29799-07-3 80%

Reaction Conditions:

at 120; for 12 h;

Steps:

2 Synthesis Example 2: Preparation of Compound 110
108 g (0.50 mol) of 1-bromoadamantane was added to 188 g (2.0 mol) of phenol, and heated at 120° C. for 12 hours. Afier the reaction was completed, the resulting solution was cooled to room temperature and stirred in a beaker containing 2 L of hot water, thereby forming a precipitate. After filtering, the precipitate was washed three times with hot water and sufficiently vacuum-dried, thereby obtaining 91.3 g of 4-(adamantane-1 -yl)phenol with a yield of 80%.

References:

MATERIAL SCIENCE CO., LTD.;JEONG, Jae Ho;LEE, Tae Wan;DO, Kwang Seok;LEE, Dong Hun;KIM, Jin Sung US2019/16666, 2019, A1 Location in patent:Paragraph 0077; 0078

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