4-(2-chlorophenyl)butanenitrile synthesis
- Product Name:4-(2-chlorophenyl)butanenitrile
- CAS Number:91552-19-1
- Molecular formula:C10H10ClN
- Molecular Weight:179.65
89-98-5
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C
2: TiCl4(2,4,6-collidine); 2,4,6-trimethyl-pyridine; manganese / tetrahydrofuran / 20 h / 70 °C / Inert atmosphere
References:
Suga, Takuya;Shimazu, Shoma;Ukaji, Yutaka [Organic Letters,2018,vol. 20,# 17,p. 5389 - 5392]
17849-38-6
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107-13-1
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6282-87-7
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30573-88-7
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