4-(2-THIENYL)BUT-3-EN-2-ONE synthesis
- Product Name:4-(2-THIENYL)BUT-3-EN-2-ONE
- CAS Number:99768-07-7
- Molecular formula:C8H8OS
- Molecular Weight:152.21
1003-31-2
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$6.00/5g
106-95-6
411 suppliers
$10.00/5g
99768-07-7
11 suppliers
$166.00/25g
Yield:99768-07-7 85%
Reaction Conditions:
Stage #1: thiophene-2-carbonitrile;allyl bromidewith zinc in tetrahydrofuran at 20; for 1 h;Cooling with ice;
Stage #2: with hydrogenchloride;water in tetrahydrofuran at 20; for 0.5 h;Cooling with ice;
References:
Chen, Fener;Hu, Chen;Huang, Zedu;Liu, Minjie;Yue, Xiaoping [Organic Process Research and Development,2020,vol. 24,# 9,p. 1700 - 1706] Location in patent:supporting information
98-03-3
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$5.00/25g
99768-07-7
11 suppliers
$166.00/25g
301164-69-2
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$48.00/1g
1730-25-2
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$66.20/100ml
99768-07-7
11 suppliers
$166.00/25g
188290-36-0
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4635-59-0
464 suppliers
$17.67/10gm:
1468-84-4
29 suppliers
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99768-07-7
11 suppliers
$166.00/25g
625-38-7
158 suppliers
$25.00/5g
99768-07-7
11 suppliers
$166.00/25g