4,4,6-TRIMETHYL-2-VINYL-1,3,2-DIOXABORINANE synthesis
- Product Name:4,4,6-TRIMETHYL-2-VINYL-1,3,2-DIOXABORINANE
- CAS Number:4627-10-5
- Molecular formula:C8H15BO2
- Molecular Weight:154.01
107-41-5
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1826-67-1
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4627-10-5
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$831.95/5G
Yield:4627-10-5 82%
Reaction Conditions:
Stage #1: vinyl magnesium bromidewith Trimethyl borate in tetrahydrofuran at -78; for 1 h;
Stage #2: with hydrogenchloride in tetrahydrofuran;diethyl ether at 20; for 0.166667 h;
Stage #3: 2-methyl-2,4-pentanediol in tetrahydrofuran;diethyl ether at 20; for 1 h;
References:
Lightfoot, Andrew P.;Twiddle, Steven J.R.;Whiting, Andrew [Organic and Biomolecular Chemistry,2005,vol. 3,# 17,p. 3167 - 3172]
107-41-5
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121-43-7
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1826-67-1
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4627-10-5
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$831.95/5G
230299-21-5
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75927-49-0
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4627-10-5
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13722-63-9
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4627-10-5
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7568-01-6
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4627-10-5
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