4-(4-METHOXYPHENYL)-1,2,3-THIADIAZOLE synthesis
- Product Name:4-(4-METHOXYPHENYL)-1,2,3-THIADIAZOLE
- CAS Number:18212-22-1
- Molecular formula:C9H8N2OS
- Molecular Weight:192.24
100-06-1
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18212-22-1
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$137.75/1g
Yield:18212-22-1 100%
Reaction Conditions:
Stage #1: 1-(4-methoxyphenyl)ethanonewith polystyrene-sulfonylhydrazide resin;acetic acid in tetrahydrofuran at 50; for 4 h;Solid phase reaction;
Stage #2: with thionyl chloride in 1,2-dichloro-ethane at 60; for 5 h;Solid phase reaction;Hurd-Mori cyclization;
References:
Hu, Yonghan;Baudart, Sylvie;Porco Jr., John A. [Journal of Organic Chemistry,1999,vol. 64,# 3,p. 1049 - 1051]
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18212-22-1
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18212-22-1
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2196-99-8
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18212-22-1
26 suppliers
$137.75/1g