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ChemicalBook CAS DataBase List (4-AMINO-PYRIDIN-3-YL)-METHANOL
138116-34-4

(4-AMINO-PYRIDIN-3-YL)-METHANOL synthesis

9synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: triethylamine / dichloromethane / 2.25 h / 0 - 20 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 3 h / -78 - 0 °C / Inert atmosphere
2.2: 0.75 h / 0 - 20 °C
3.1: hydrogenchloride; water / 8 h / Reflux
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 20 °C

References:

GRÜNENTHAL GMBH;FRANK, Robert;CHRISTOPH, Thomas;LESCH, Bernhard;LEE, Jeewoo WO2013/13817, 2013, A1

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