(4-AMINO-PYRIDIN-3-YL)-METHANOL synthesis
- Product Name:(4-AMINO-PYRIDIN-3-YL)-METHANOL
- CAS Number:138116-34-4
- Molecular formula:C6H8N2O
- Molecular Weight:124.14
504-24-5
488 suppliers
$10.00/1 g
138116-34-4
110 suppliers
$26.00/100mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: triethylamine / dichloromethane / 2.25 h / 0 - 20 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 3 h / -78 - 0 °C / Inert atmosphere
2.2: 0.75 h / 0 - 20 °C
3.1: hydrogenchloride; water / 8 h / Reflux
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 20 °C
References:
GRÜNENTHAL GMBH;FRANK, Robert;CHRISTOPH, Thomas;LESCH, Bernhard;LEE, Jeewoo WO2013/13817, 2013, A1
42373-30-8
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138116-34-4
110 suppliers
$26.00/100mg
16135-36-7
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$9.00/1g
138116-34-4
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$26.00/100mg
1003-73-2
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$9.00/5g
138116-34-4
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1074-98-2
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$14.00/5g
138116-34-4
110 suppliers
$26.00/100mg