ChemicalBook CAS DataBase List 4-Biphenylacetonitrile

4-Biphenylacetonitrile synthesis

12synthesis methods

Product Name:4-Biphenylacetonitrile
CAS Number:31603-77-7
Molecular formula:C14H11N
Molecular Weight:193.24

773837-37-9 Synthesis

773837-37-9
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1667-11-4 Synthesis

1667-11-4
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31603-77-7
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Yield: 173.7 g

Reaction Conditions:

in water at 70 - 75; for 4 h;Time;

Steps:

3
1000 ml four bottles into the 500g water,182.2 g Biphenyl monochlorobenzyl chloride,44.1 g of sodium cyanide,Heating to 70 ~ 75 between the incubation reaction 4 hours,Cooled to room temperature and filtered to give 173.7 g of 4-biphenylacetonitrile,Water is treated with hydrogen peroxide.

References:

Huangshi Lifuda Pharmaceutical Chemical Co., Ltd.;Cheng, Jiagang CN106431911, 2017, A Location in patent:Paragraph 0063; 0066; 0073; 0080

16532-79-9 Synthesis