4'-(Dimethylamino)-[1,1'-biphenyl]-4-carbaldehyde synthesis

8synthesis methods

Product Name:4'-(Dimethylamino)-[1,1'-biphenyl]-4-carbaldehyde
CAS Number:173991-06-5
Molecular formula:C15H15NO
Molecular Weight:225.29

15164-44-0
292 suppliers
$6.00/1g

4-(N,N-DIMETHYLAMINO)PHENYLBORONIC ACID, PINACOL ESTER

171364-78-6
129 suppliers
$8.00/250mg

4'-(Dimethylamino)-[1,1'-biphenyl]-4-carbaldehyde

173991-06-5
23 suppliers
$233.59/100mg

Yield:173991-06-5 90%

Reaction Conditions:

with [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II);anhydrous sodium carbonate in tetrahydrofuran;lithium hydroxide monohydrate at 60; for 12 h;Inert atmosphere;Schlenk technique;Suzuki-Miyaura Coupling;

References:

Klikar, Milan;Bures, Filip;Pytela, Oldrich;Mikysek, Tomas;Padelkova, Zdenka;Barsella, Alberto;Dorkenoo, Kokou;Achelle, Sylvain [New Journal of Chemistry,2013,vol. 37,# 12,p. 4230 - 4240] Location in patent:supporting information

586-77-6 Synthesis