Welcome to chemicalbook!
Chinese English Japanese Germany Korea
010-86108875
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List 4-(FLUOROSULFONYL)BENZOYL CHLORIDE
402-55-1

4-(FLUOROSULFONYL)BENZOYL CHLORIDE synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: tetrafluoroboric acid; tert.-butylnitrite / ethanol; water / 1 h / 0 - 20 °C
1.2: 9 h / 70 °C / Schlenk technique; Inert atmosphere
2.1: thionyl chloride / 75 °C

References:

Zhong, Tao;Pang, Meng-Ke;Chen, Zhi-Da;Zhang, Bin;Weng, Jiang;Lu, Gui [Organic Letters,2020,vol. 22,# 8,p. 3072 - 3078]