4-MethylpentanaMide synthesis
- Product Name:4-MethylpentanaMide
- CAS Number:1119-29-5
- Molecular formula:C6H13NO
- Molecular Weight:115.17
Yield:1119-29-5 144 g
Reaction Conditions:
with sodium ethanolate in ethanol at 50 - 65;
Steps:
1 Preparation of 2-isobutylacetoacetamide
the reactor, are sequentially added 4.5mol anhydrous ethanol, 1mol acetamide, 1.1mol sodium ethoxide and 1.1mol isobutyl bromide, controlling the reaction temperature is 65 °C, stirring the reaction is complete, a distillation recovery ethanol, water heating to dissolve the distillation residue, filtration, filtrate cooling, separating out 2-isobutyl-acetamide, drying the compound 144 g.
References:
CN103709054,2016,B Location in patent:Paragraph 0009
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