4-Oxooctanoic acid ethyl ester synthesis
- Product Name:4-Oxooctanoic acid ethyl ester
- CAS Number:37174-96-2
- Molecular formula:C10H18O3
- Molecular Weight:186.25
Yield:37174-96-2 74%
Reaction Conditions:
Stage #1: butyl magnesium bromidewith tributylphosphine in tetrahydrofuran at 20;
Stage #2: ethyl 3-(chloroformyl)propionate in tetrahydrofuran at -40; for 0.333333 h;
References:
Maeda;Hino;Yamauchi;Ohmori [Chemical and Pharmaceutical Bulletin,2000,vol. 48,# 8,p. 1196 - 1199]
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