4-(P-IODOPHENYL)BUTYRIC ACID synthesis
- Product Name:4-(P-IODOPHENYL)BUTYRIC ACID
- CAS Number:27913-58-2
- Molecular formula:C10H11IO2
- Molecular Weight:290.1
589-87-7
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27913-58-2
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$21.00/250mg
Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere
1.2: -78 °C / Inert atmosphere
2.1: tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
3.1: chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); lithium methanolate / tetrahydrofuran / 24 h / 70 °C / 760.05 Torr / Inert atmosphere
3.2: Inert atmosphere
References:
Ohishi, Takeshi;Zhang, Liang;Nishiura, Masayoshi;Hou, Zhaomin [Angewandte Chemie - International Edition,2011,vol. 50,# 35,p. 8114 - 8117]
1821-12-1
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27913-58-2
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$21.00/250mg
124-38-9
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$175.00/23402
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1000210-73-0
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27913-58-2
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$21.00/250mg
194146-02-6
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$303.00/1g
27913-58-2
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591-50-4
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$10.00/1g
27913-58-2
79 suppliers
$21.00/250mg