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4-(propylamino)benzoic acid(SALTDATA: FREE) synthesis

5synthesis methods
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Yield:73686-77-8 70%

Reaction Conditions:

Stage #1: 4-amino-benzoic acid;propionaldehydewith borane-2-picoline complex in methanol at 20; for 14 h;
Stage #2: in methanol;

References:

Campbell, Fred;Kilner, Colin A.;Wilson, Andrew J. [Tetrahedron Letters,2010,vol. 51,# 10,p. 1361 - 1363] Location in patent:supporting information; experimental part