1-(1-hydroxyphenyl)-3-(4-methoxyphenyl)propane-1,3-dione synthesis
- Product Name:1-(1-hydroxyphenyl)-3-(4-methoxyphenyl)propane-1,3-dione
- CAS Number:4143-72-0
- Molecular formula:C16H14O4
- Molecular Weight:270.28
5445-86-3
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Yield:4143-72-0 97%
Reaction Conditions:
Stage #1: 2'-(4-methoxybenzoyloxy)acetophenonewith pyridineBaker-Venkataraman Rearrangement;
Stage #2: with potassium hydroxide at 50;Baker-Venkataraman Rearrangement;
References:
Paez, Elida Betania Ariza;Curcio, Sergio;Neme, Natália P.;Matos, Matheus J. S.;Correa, Rodrigo S.;Pereira, Fabio Junio;Hilário, Flaviane Francisco;Cazati, Thiago;Taylor, Jason Guy [New Journal of Chemistry,2020,vol. 44,# 34,p. 14615 - 14631] Location in patent:supporting information
![1-[2-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]phenyl]-3-(4-methoxyphenyl)-1,3-propanedione](/CAS/20210305/GIF/136003-87-7.gif)
136003-87-7
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4143-72-0
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