ChemicalBook CAS DataBase List tert-Butyl 9-oxo-3-oxa-7-azabicyclo[3.3.1]nonane-7-carboxylate

tert-Butyl 9-oxo-3-oxa-7-azabicyclo[3.3.1]nonane-7-carboxylate synthesis

4synthesis methods

Product Name:tert-Butyl 9-oxo-3-oxa-7-azabicyclo[3.3.1]nonane-7-carboxylate
CAS Number:454695-20-6
Molecular formula:C12H19NO4
Molecular Weight:241.28

29943-42-8 Synthesis

29943-42-8
419 suppliers
$5.00/1g

tert-Butyl 9-oxo-3-oxa-7-azabicyclo[3.3.1]nonane-7-carboxylate

454695-20-6
52 suppliers
$459.51/5MG

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: 75 percent / AcOH / methanol / 1 h / 65 °C
2.1: ClCOOCH(Cl)CH₃ / CH₂Cl₂ / 2 h / Heating
2.2: MeOH / 1 h / Heating
3.1: 456 mg / aq. KOH / dioxane / 12 h / 20 °C

References:

Huttenloch, Oliver;Laxman, Eltepu;Waldmann, Herbert [Chemistry - A European Journal,2002,vol. 8,# 20,p. 4767 - 4780]

FullText

24424-99-5 Synthesis

24424-99-5
816 suppliers
$13.50/25G

3-Benzyl-7-oxo-3-aza-bicyclo[3.3.1nonan-9-one

77716-01-9
64 suppliers
$60.00/100mg

454695-20-6
52 suppliers
$459.51/5MG

References

24424-99-5 Synthesis

24424-99-5
816 suppliers
$13.50/25G

57155-42-7
3 suppliers
inquiry

454695-20-6
52 suppliers
$459.51/5MG

References

77716-01-9
64 suppliers
$60.00/100mg

454695-20-6
52 suppliers
$459.51/5MG

References