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152920-53-1

5-(3-THIENYL)-1H-INDOLE synthesis

4synthesis methods
6165-69-1 Synthesis
3-Thiopheneboronic acid

6165-69-1
343 suppliers
$12.72/1gm:

17422-32-1 Synthesis
5-Chloroindole

17422-32-1
376 suppliers
$6.00/1g

5-(3-THIENYL)-1H-INDOLE

152920-53-1
16 suppliers
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Yield:152920-53-1 90%

Reaction Conditions:

with potassium phosphate;dicyclohexylphosphino-2′,4′,6′-triisopropylbiphenyl;tris(dibenzylideneacetone)dipalladium (0) in butan-1-ol at 100; for 15 h;Suzuki-Miyaura coupling;

References:

Billingsley, Kelvin;Buchwald, Stephen L. [Journal of the American Chemical Society,2007,vol. 129,# 11,p. 3358 - 3366]