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ChemicalBook CAS DataBase List 5-(4 4 5 5-TETRAMETHYL-1 3 2-DIOXABOROL&

5-(4 4 5 5-TETRAMETHYL-1 3 2-DIOXABOROL& synthesis

11synthesis methods
-

Yield:479719-88-5 94%

Reaction Conditions:

Stage #1: 2,2'-Bithiophenewith n-butyllithium in tetrahydrofuran at -78 - 20; for 1.58333 h;Inert atmosphere;
Stage #2: 2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane at -78 - 20;

References:

Haid, Stefan;Marszalek, Magdalena;Mishra, Amaresh;Wielopolski, Mateusz;Teuscher, Joel;Moser, Jacques-E.;Humphry-Baker, Robin;Zakeeruddin, Shaik M.;Graetzel, Michael;Baeuerle, Peter [Advanced Functional Materials,2012,vol. 22,# 6,p. 1291 - 1302] Location in patent:experimental part

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