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5-Benzoyl-M-xylene synthesis

13synthesis methods
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Yield:13319-70-5 99.1%

Reaction Conditions:

with oxygen at 110; for 8 h;Sealed tube;

Steps:

19 Example 19: Synthesis of 3,5-Dimethylbenzophenone

Add 0.5mmol of 1,3-dimethyl-5-(1-phenylvinyl)benzene and 1mL polyethylene glycol dimethyl ether (MW=250) into a test tube as a solvent, seal the test tube, and perform oxygen After replacement, a balloon filled with pure oxygen was inserted, and the reaction was kept at 110°C for 8 hours. The yield was 99.1%.

References:

CN112608222,2021,A Location in patent:Paragraph 0019