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ChemicalBook CAS DataBase List 5-Hydroxy-1,4-naphthalenedione

5-Hydroxy-1,4-naphthalenedione synthesis

14synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 82 percent / Et3N / 4-dimethylaminopiridine / acetone / 2 h / Ambient temperature
2: 71 percent / H2 / Pd/C
3: 78 percent / methylene blue, O2 / acetonitrile / 4 h / 20 °C / Irradiation

References:

Mohrle;Folttmann [Archiv der Pharmazie,1988,vol. 321,# 3,p. 167 - 170]

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