5-Methoxy-4-chromanone synthesis
- Product Name:5-Methoxy-4-chromanone
- CAS Number:863309-86-8
- Molecular formula:C10H10O3
- Molecular Weight:178.18
49855-03-0
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42327-52-6
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863309-86-8
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$377.00/250mg
Yield:863309-86-8 67%
Reaction Conditions:
with PPA at 67; for 1 h;
Steps:
1; 3
3-(2-Methoxyphenoxy)propanoic acid (5.61 mmol) and polyphosphoric (25 ml_) are combined and heated at 67 0C for 1 h. The reaction mixture is diluted with ice water (150 ml_) and the precipitated solids are collected by filtration, washed with water, and dried to provide 8-methoxy-2,3-dihydrochromen-4-one (Target C2) in 67% yield as a brown solid.
References:
WO2009/55437,2009,A2 Location in patent:Page/Page column 59; 60
150-19-6
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863309-86-8
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$377.00/250mg
703-23-1
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863309-86-8
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59887-87-5
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863309-86-8
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6279-84-1
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863309-86-8
35 suppliers
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