ethyl 5-nitro-2,6-dioxo-3H-pyrimidine-4-carboxylate synthesis

3synthesis methods

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 91 percent / fuming HNO₃ (d 1.5) / 4 h / 100 °C
2: 97 percent / conc. H₂SO₄ / 9 h / Heating

References:

Boyle, Peter H.;Gillespie, Paul [Journal of Chemical Research, Miniprint,1989,# 9,p. 2086 - 2097]

64-17-5 Synthesis

65-86-1 Synthesis

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