5-ACETYL-6-METHYL-2-OXO-1,2-DIHYDRO-3-PYRIDINECARBOXAMIDE synthesis
- Product Name:5-ACETYL-6-METHYL-2-OXO-1,2-DIHYDRO-3-PYRIDINECARBOXAMIDE
- CAS Number:52600-60-9
- Molecular formula:C9H10N2O3
- Molecular Weight:194.19
52600-53-0
48 suppliers
inquiry
52600-60-9
17 suppliers
$244.00/500mg
Yield:-
Reaction Conditions:
with sulfuric acid
Steps:
16 5-Acetyl-1,2-Dihydro-6-Methyl-2-Oxo-3-Pyridinecarboxamide
EXAMPLE 16 5-Acetyl-1,2-Dihydro-6-Methyl-2-Oxo-3-Pyridinecarboxamide To 100 grams of concentrated sulfuric acid is added 10 g (0.056 mole) of 5-acetyl-1,2-dihydro-6-methyl-2-oxo-3-pyridinecarbonitrile. The mixture is stirred at 60° C. for 5 hours, cooled and then poured on 1 kg ice. The resulting solid is collected, washed with water and recrystallized from ethanol to give the title compound.
References:
US4568751,1986,A US4732982,1988,A
4637-24-5
646 suppliers
$5.00/25g
123-54-6
588 suppliers
$10.00/25ml
107-91-5
579 suppliers
$5.00/10g
52600-53-0
48 suppliers
inquiry
52600-60-9
17 suppliers
$244.00/500mg
![2,4-Pentanedione, 3-[(dimethylamino)methylene]-](/CAS/GIF/18856-72-9.gif)
18856-72-9
10 suppliers
inquiry
107-91-5
579 suppliers
$5.00/10g
52600-60-9
17 suppliers
$244.00/500mg
33884-41-2
35 suppliers
$66.89/5g
52600-60-9
17 suppliers
$244.00/500mg
18856-72-9
10 suppliers
inquiry
52600-60-9
17 suppliers
$244.00/500mg