6-CHLORO-2-METHYL-9H-PURINE synthesis
- Product Name:6-CHLORO-2-METHYL-9H-PURINE
- CAS Number:100859-35-6
- Molecular formula:C6H5ClN4
- Molecular Weight:168.58
933-80-2
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Yield:100859-35-6 93%
Reaction Conditions:
at 100; for 1.5 h;
Steps:
147.2 Step 2.
A solution of 6-chloro-2-methylpyrimidine-4,5-diamine (810 mg, 5.13 mmol) in triethoxymethane (10 mL) was stirred at 100 °C for 1.5 hours. The mixture was concentrated to afford 6-chloro-2-methyl-9H-purine (800 mg, 4.76 mmol, 93%) as a yellow solid. MS (ESI) m/z 169.1 [M+H]+
References:
WO2022/178256,2022,A1 Location in patent:Paragraph 1192
676-58-4
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18552-90-4
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5167-18-0
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933-80-2
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$91.00/100mg
149-73-5
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39906-04-2
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