6-Ethoxy-nicotinic acid methyl ester synthesis
- Product Name:6-Ethoxy-nicotinic acid methyl ester
- CAS Number:74357-22-5
- Molecular formula:C9H11NO3
- Molecular Weight:181.19
51105-90-9
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74357-22-5
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$964.00/1g
Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 20 °C / Inert atmosphere
1.2: 0.5 h / 20 °C / Inert atmosphere
2.1: sodium periodate / dichloromethane / 2 h / 22 °C / Inert atmosphere
2.2: Inert atmosphere
3.1: 5,5-dimethyl-1,3-cyclohexadiene / 24 h / 140 °C
References:
Anderson, Erin D.;Boger, Dale L. [Journal of the American Chemical Society,2011,vol. 133,# 31,p. 12285 - 12292]
66171-50-4
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75-03-6
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$11.00/5g
74357-22-5
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$964.00/1g
875554-08-8
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74357-22-5
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93-60-7
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64-17-5
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74357-22-5
10 suppliers
$964.00/1g
74357-20-3
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74357-21-4
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