Trimethylsilylketene Ethyl Trimethylsilyl Acetal (mixture of isomers) synthesis
- Product Name:Trimethylsilylketene Ethyl Trimethylsilyl Acetal (mixture of isomers)
- CAS Number:65946-56-7
- Molecular formula:C10H24O2Si2
- Molecular Weight:232.47
4071-88-9
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$21.00/1g
18162-48-6
692 suppliers
$9.00/5g
65946-56-7
26 suppliers
$130.00/500mg
Yield:65946-56-7 93%
Reaction Conditions:
Stage #1: trimethylsilanyl-acetic acid ethyl esterwith lithium diisopropyl amide in tetrahydrofuran at -78;
Stage #2: tert-butyldimethylsilyl chloride in tetrahydrofuran at -78;Further stages.;
References:
Michida, Makoto;Mukaiyama, Teruaki [Chemistry Letters,2008,vol. 37,# 7,p. 704 - 705]
75-77-4
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$5.04/10
4071-88-9
152 suppliers
$21.00/1g
65946-56-7
26 suppliers
$130.00/500mg
27607-77-8
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$10.00/5g
141-78-6
652 suppliers
$24.69/250ml
4071-88-9
152 suppliers
$21.00/1g
65946-56-7
26 suppliers
$130.00/500mg
65946-55-6
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