2-ChloroMethyl-4-Methoxy-3,5-diMethylpyridine 1-Oxide synthesis
- Product Name:2-ChloroMethyl-4-Methoxy-3,5-diMethylpyridine 1-Oxide
- CAS Number:848694-10-0
- Molecular formula:C9H12ClNO2
- Molecular Weight:201.65
86604-75-3
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848694-10-0
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Yield: 90.4%
Reaction Conditions:
Stage #1:2-(chloromethyl)-4-methoxy-3,5-dimethylpyridine hydrochloride with sodium hydroxide in chloroform for 0.5 h;
Stage #2: with 3-chloro-benzenecarboperoxoic acid in chloroform at 55 - 60; for 1.5 h;Further stages.;
References:
Reddy, Ganta Madhusudhan;Prasada Raju;Babu, J. Moses;Praveen;Khunt, Mayur;Mukkanti;Pratap Reddy, Padi [Synthetic Communications,2008,vol. 38,# 11,p. 1725 - 1736]