1-(TERT-BUTYL) 6-METHYL 3-IODO-1H-INDOLE-1,6-DICARBOXYLATE synthesis
- Product Name:1-(TERT-BUTYL) 6-METHYL 3-IODO-1H-INDOLE-1,6-DICARBOXYLATE
- CAS Number:850374-94-6
- Molecular formula:C15H16INO4
- Molecular Weight:401.2
850374-98-0
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$120.00/250mg
24424-99-5
811 suppliers
$13.50/25G
850374-94-6
17 suppliers
$109.00/250mg
Yield:850374-94-6 89%
Reaction Conditions:
with dmap;triethylamine in dichloromethane at 20; for 2 h;
Steps:
5.3 Preparation of Compound 33
The 0.2g3- iodo -1H- indole-6-carboxylate was dissolved in 20mL of dichloromethane was added Boc anhydride 0.16g, 0.28mL triethylamine, 10mg4- dimethylaminopyridine were reacted at room temperature 2h, the reaction Bi, diluted with dichloromethane and washed with 5% aqueous sodium metabisulphite solution washed twice with water, brine, dried over anhydrous sodium sulfate, and rotary products done 238mg, yield 89%.
References:
CN103864753,2016,B Location in patent:Paragraph 0125; 0132-0133
850374-98-0
35 suppliers
$120.00/250mg
850374-94-6
17 suppliers
$109.00/250mg
50820-65-0
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$6.00/1g
850374-94-6
17 suppliers
$109.00/250mg
1670-82-2
346 suppliers
$10.00/1g
850374-94-6
17 suppliers
$109.00/250mg