9-(2-Ethylhexyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole synthesis
- Product Name:9-(2-Ethylhexyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole
- CAS Number:856422-41-8
- Molecular formula:C26H36BNO2
- Molecular Weight:405.38
61676-62-8
328 suppliers
$11.19/5G
628336-85-6
25 suppliers
$125.00/1G
856422-41-8
18 suppliers
$92.00/200mg
Yield:856422-41-8 89%
Reaction Conditions:
Stage #1: 3-bromo-9-(2-ethylhexyl)-9H-carbazolewith n-butyllithium in tetrahydrofuran;hexane at -78 - 20; for 2 h;Inert atmosphere;
Stage #2: 2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran;hexane at 20;Inert atmosphere;
References:
Paramasivam, Mahalingavelar;Gupta, Akhil;Raynor, Aaron M.;Bhosale, Sheshanth V.;Bhanuprakash;Jayathirtha Rao [RSC Advances,2014,vol. 4,# 67,p. 35318 - 35331]
628336-85-6
25 suppliers
$125.00/1G
73183-34-3
593 suppliers
$6.00/5g
856422-41-8
18 suppliers
$92.00/200mg
86-74-8
342 suppliers
$10.00/5g
856422-41-8
18 suppliers
$92.00/200mg
18908-66-2
298 suppliers
$5.00/25g
856422-41-8
18 suppliers
$92.00/200mg
1592-95-6
407 suppliers
$5.00/1g
856422-41-8
18 suppliers
$92.00/200mg