1,3-Dihydro-3,3-dimethyl-1-(trifluoromethyl)-1,2-benziodoxole, Tognis Reagent synthesis
- Product Name:1,3-Dihydro-3,3-dimethyl-1-(trifluoromethyl)-1,2-benziodoxole, Tognis Reagent
- CAS Number:887144-97-0
- Molecular formula:C10H10F3IO
- Molecular Weight:330.09
610-97-9
422 suppliers
$9.00/1g
887144-97-0
168 suppliers
$28.00/250mg
Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: diethyl ether / 3 h / 0 - 23 °C / Inert atmosphere
1.2: 1 h / 23 °C / Inert atmosphere
2.1: acetonitrile / 16 h / 23 °C / Inert atmosphere; Darkness
3.1: cesium fluoride / acetonitrile / 16 h / 23 °C / Inert atmosphere; Darkness
References:
Powers, David C.;Lee, Eunsung;Ariafard, Alireza;Sanford, Melanie S.;Yates, Brian F.;Canty, Allan J.;Ritter, Tobias [Journal of the American Chemical Society,2012,vol. 134,# 29,p. 12002 - 12009]
69352-04-1
33 suppliers
$205.00/10g
81290-20-2
417 suppliers
$13.00/1g
887144-97-0
168 suppliers
$28.00/250mg
69352-04-1
33 suppliers
$205.00/10g
75-46-7
0 suppliers
$150.00/50 g
887144-97-0
168 suppliers
$28.00/250mg
81290-20-2
417 suppliers
$13.00/1g
175786-58-0
4 suppliers
inquiry
887144-97-0
168 suppliers
$28.00/250mg
1391728-13-4
42 suppliers
$20.00/100mg
81290-20-2
417 suppliers
$13.00/1g
887144-97-0
168 suppliers
$28.00/250mg