4-Pentenoicacid,2-amino-2-methyl-,methylester,(2S)-(9CI) synthesis
- Product Name:4-Pentenoicacid,2-amino-2-methyl-,methylester,(2S)-(9CI)
- CAS Number:88820-87-5
- Molecular formula:C7H13NO2
- Molecular Weight:143.18
![L-Alanine, N-[(4-chlorophenyl)methylene]-, methyl ester](/CAS/20210305/GIF/91292-73-8.gif)
Yield:91 % ee
Reaction Conditions:
with tetrakis(triphenylphosphine) palladium(0);tetrakis(acetonitrile)copper(I)tetrafluoroborate;(S,S)-iPr-Foxap;triethyl borane;magnesium sulfate in tetrahydrofuran at 15;Schlenk technique;Inert atmosphere;
References:
Xiao, Lu;Chang, Xin;Xu, Hui;Xiong, Qi;Dang, Yanfeng;Wang, Chun-Jiang [Angewandte Chemie - International Edition,2022,vol. 61,# 46,art. no. E202212948][Angew. Chem.,2022,vol. 134,# 46] Location in patent:supporting information
![METHYL 2-([(E)-PHENYLMETHYLIDENE]AMINO)PROPANOATE](/StructureFile/ChemBookStructure7/GIF/CB0365181.gif)
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