5-ACETYL-2-AMINO-6-METHYL-4-PHENYL-4H-PYRAN-3-CARBONITRILE synthesis
- Product Name:5-ACETYL-2-AMINO-6-METHYL-4-PHENYL-4H-PYRAN-3-CARBONITRILE
- CAS Number:89809-89-2
- Molecular formula:C15H14N2O2
- Molecular Weight:254.28
100-52-7
977 suppliers
$21.30/2g
105-45-3
692 suppliers
$5.00/5g
109-77-3
455 suppliers
$10.00/5g
89809-89-2
20 suppliers
$30.00/20mg
Yield:89809-89-2 96%
Reaction Conditions:
with Ferric Sulfasalazine Sulfa Drug Complex Supported on Cobalt Ferrite Cellulose in ethanol at 60; for 0.15 h;
Steps:
2.3 General Procedure for the 4H- Pyrans Derivatives Synthesis
General procedure: A suspension of malonitrile (1mmol), ethyl acetoacetate(methyl acetoacetate, acetoacetate) (1mmol), aldehyde(1mmol) and the catalyst (0.01g, 0.0016mmol) in ethanol(10ml) was stirred at 60°C. After completion of the reactionwhich was monitored by TLC, the catalyst was separatedby using an external magnet. The mixture was poured into cold water and the precipitate was filtered. The solid wasrecrystallized with ethanol and dried in an oven at 60°C.
References:
Rostamizadeh, Shahnaz;Daneshfar, Zahra;Khazaei, Ali [Catalysis Letters,2020,vol. 150,# 7,p. 2091 - 2114]
100-52-7
977 suppliers
$21.30/2g
123-54-6
588 suppliers
$10.00/25ml
109-77-3
455 suppliers
$10.00/5g
89809-89-2
20 suppliers
$30.00/20mg
2700-22-3
124 suppliers
$14.00/1g
123-54-6
588 suppliers
$10.00/25ml
89809-89-2
20 suppliers
$30.00/20mg
4335-90-4
62 suppliers
$28.60/250mg
109-77-3
455 suppliers
$10.00/5g
89809-89-2
20 suppliers
$30.00/20mg
2700-22-3
124 suppliers
$14.00/1g
123-54-6
588 suppliers
$10.00/25ml
89809-89-2
20 suppliers
$30.00/20mg
![4H-Pyrano[2,3-b]pyridine-6,6(7H)-dicarbonitrile, 3-acetyl-5-amino-2-methyl-4,7-diphenyl-](/CAS/20210305/GIF/115041-50-4.gif)
115041-50-4
0 suppliers
inquiry