9-DECEN-1-OL synthesis
- Product Name:9-DECEN-1-OL
- CAS Number:13019-22-2
- Molecular formula:C10H20O
- Molecular Weight:156.27
112-47-0
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13019-22-2
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Yield:13019-22-2 88%
Reaction Conditions:
with 1-hexadecylcarboxylic acid at 340; for 5 h;Molecular sieve;Temperature;Reagent/catalyst;
Steps:
1-1 Synthesis of 9-decenol (Cyclic reaction)
18 g of the vacuum distillation bottoms liquid obtained in the step 2) of Example 1 was mixed with fresh raw material - 1,10-decanediol (which may be mixed in any ratio), and the resulting mixture was used in place of that used in the step 1) 1, 10-decanediol was continuously fed and then the reaction was continued according to the process conditions of step 1) of Example 1; namely, the discharge rate was adjusted to 30 g / h, and the feed rate was adjusted to be consistent with the discharge rate .The reaction was continued for 6 hours, feeding 190 g and discharging about 180 g.And then subjected to atmospheric distillation and vacuum distillation as in Example 1, step 2) to obtain 9-decenol, yield 88%, and purity 99.3%.Based on the above data, we know that the above-mentioned cyclic reaction does not affect the final yield and product purity.
References:
Chemipanda Bio-Tech Co.,Ltd;Lai, Yifeng;Li, Shouming;Zhang, Heng CN105330516, 2016, A Location in patent:Paragraph 0039; 0040
25601-41-6
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13019-22-2
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14436-32-9
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13019-22-2
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67233-91-4
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13019-22-2
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