Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
logo
Inquriy
Try our best to find the right business for you.
Messages
Do not miss inquiry messages Please log in to view all inquiry messages.
My chemicalbook

Welcome back!

Structured search
18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 4-([6-(METHACRYLOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID
91652-00-5

4-([6-(METHACRYLOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID synthesis

9synthesis methods
The preparation of 4-([6-(methacryloyloxy)hexyl]oxy)benzenecarboxylic acid is as follows:6-(4-Formylphenoxy)hexyl methacrylate in an amount of 116.14 g, 2100 mL of methanol, an aqueous sodium dihydrogen phosphate solution (obtained by dissolving 43 g of sodium dihydrogen phosphate dihydrate in 570 mL of water) and 73 mL of a 30% hydrogen peroxide solution were added one by one. An aqueous sodium chlorite solution (obtained by dissolving 61.9 g of sodium chlorite with the purity of 80% in 500 mL of water) was added by dropping. After dropping, the reaction liquid was stirred at 45° C. for 3 hours, and the reaction was finished. After slowly cooling the reaction liquid to 20° C., 2250 mL of water was dropped to the reaction liquid, and a solid was precipitated. The solid was collected by filtration, and 72.7 g of 4-((6-(methacryloyloxy)hexyl)oxy)benzoic acid was thus obtained.

91652-00-5.png

2009-83-8 Synthesis
6-Chlorohexanol

2009-83-8
380 suppliers
$7.00/25g

4-([6-(METHACRYLOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID

91652-00-5
44 suppliers
inquiry

-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: NaOH, KI
2: C5H5N

References:

Mariam, Yitbarek H.;Pemawansa, Kariyawasam P. W.;Okoh, Fred;Bota, Kofi B. [Molecular Crystals and Liquid Crystals (1969-1991),1986,vol. 141,p. 77 - 96]

4-(6-HYDROXYHEXYLOXY)BENZOIC ACID

83883-25-4
58 suppliers
$79.00/1G

Methacryloyl chloride

920-46-7
343 suppliers
$20.00/1g

4-([6-(METHACRYLOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID

91652-00-5
44 suppliers
inquiry

References
760-93-0 Synthesis
Methacrylic anhydride

760-93-0
328 suppliers
$28.46/50g

4-(6-HYDROXYHEXYLOXY)BENZOIC ACID

83883-25-4
58 suppliers
$79.00/1G

4-([6-(METHACRYLOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID

91652-00-5
44 suppliers
inquiry

References
6-Bromo-1-hexanol

4286-55-9
303 suppliers
$15.00/10g

4-([6-(METHACRYLOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID

91652-00-5
44 suppliers
inquiry

References
99-76-3 Synthesis
Methylparaben

99-76-3
784 suppliers
$5.00/25g

4-([6-(METHACRYLOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID

91652-00-5
44 suppliers
inquiry

References

4-([6-(METHACRYLOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID Related Search:

Phosphorus 4-((6-(Acryloyloxy)hexyl)oxy)benzoic acid