2-(5-Hexyl-2-thienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane synthesis
- Product Name:2-(5-Hexyl-2-thienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
- CAS Number:917985-54-7
- Molecular formula:C16H27BO2S
- Molecular Weight:294.26
61676-62-8
329 suppliers
$11.19/5G
211737-28-9
104 suppliers
$15.00/250mg
917985-54-7
81 suppliers
$60.00/100mg
Yield:917985-54-7 100%
Reaction Conditions:
Stage #1: 2-bromo-5-hexylthiophenewith n-butyllithium in tetrahydrofuran at -70; for 0.75 h;
Stage #2: 2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran at 25; for 18 h;
References:
Bomben, Paolo G.;Gordon, Terry J.;Schott, Eduardo;Berlinguette, Curtis P. [Angewandte Chemie - International Edition,2011,vol. 50,# 45,p. 10682 - 10685] Location in patent:supporting information; experimental part
18794-77-9
209 suppliers
$8.00/1g
61676-62-8
329 suppliers
$11.19/5G
917985-54-7
81 suppliers
$60.00/100mg
18794-77-9
209 suppliers
$8.00/1g
25015-63-8
225 suppliers
$22.39/5G
917985-54-7
81 suppliers
$60.00/100mg
73183-34-3
591 suppliers
$6.00/5g
211737-28-9
104 suppliers
$15.00/250mg
917985-54-7
81 suppliers
$60.00/100mg
111-25-1
323 suppliers
$10.00/5g
917985-54-7
81 suppliers
$60.00/100mg