Allyl acetate synthesis
- Product Name:Allyl acetate
- CAS Number:591-87-7
- Molecular formula:C5H8O2
- Molecular Weight:100.12
Allyl acetate is produced primarily for manufacturing allyl alcohol. It is also used as a synthetic flavoring for cheese, butter, and fruit.
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591-87-7
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Yield:591-87-7 98.1%
Reaction Conditions:
with triethylamine in dichloromethane at 5 - 20; for 4 h;
Steps:
2 Preparation of 3 - Acetoxypropylene
To a 1000 ml reaction flask was added 400 g of methylene chloride, 58.0 g (1.0 mol) of propenol and 82.5 g (1.05 mol) of acetyl chloride, cooled to minus 5 ° C, and 106.0 g of triethylamine The reaction was allowed to warm to 20 ° C for 4 hours. After completion of the reaction, the mixture was filtered off and the filtrate was washed with 50 g of methylene chloride. The filtrate was combined and the methylene chloride was recovered at atmospheric pressure and distilled under reduced pressure (65-72 ° C / 15 mm Hg) to obtain 98.1 Grams of colorless transparent liquid 3-acetoxypropylene, the yield of 98. 1%.
References:
CN104163808,2016,B Location in patent:Paragraph 0072; 0073
64-19-7
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591-87-7
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591-87-7
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64-19-7
1518 suppliers
$10.00/25ML
591-87-7
178 suppliers
$10.00/10g