ChemicalBook CAS DataBase List Amlodipine Impurity 27 Disodium Salt

Amlodipine Impurity 27 Disodium Salt synthesis

1synthesis methods

Product Name:Amlodipine Impurity 27 Disodium Salt
CAS Number:120289-11-4
Molecular formula:C19H20ClNO7
Molecular Weight:409.82

89-98-5 Synthesis

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 2.17 g / piperidine / methanol / 1.) 16 h, RT, 2.) 6 h, reflux
2: 0.72 percent / NaOH / H₂O; 1,2-dimethoxy-ethane / 7 h / Ambient temperature

References:

Beresford;Macrae;Alker;Kobylecki [Arzneimittel-Forschung/Drug Research,1989,vol. 39,# 2,p. 201 - 209]

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