AMYL LACTATE synthesis
- Product Name:AMYL LACTATE
- CAS Number:6382-06-5
- Molecular formula:C8H16O3
- Molecular Weight:160.21
Yield:-
Reaction Conditions:
with titanium-silicon molecular sieve TS-2;Sn-Ti-MFI-2 molecular sieve at 160; for 17 h;Sealed tube;
Steps:
5 Example 5
Weigh 0.15g of the tin-silicon molecular sieve Sn-MFI prepared in Preparation Example 1 and 0.15g of the titanium-silicon molecular sieve Ti-Beta prepared in Preparation Example 6 as a catalyst in a 100mL polytetrafluoroethylene lining, and then sequentially add 8g of amyl alcohol , 0.1g mannose. The polytetrafluoroethylene liner was placed in a stainless steel reactor and sealed, and placed in a homogeneous reactor to start the reaction. The reaction temperature was controlled at about 160°C and the reaction was carried out for 17 hours. The specific reaction results are shown in Table 1.
References:
Sinopec Corporation;Sinopec Corporation Petrochemical Sciences Institute;Lin Min;Liu Yujia;Xia Changjiu;Zhu Bin;Yang Yongjia;Peng Xinxin;Luo Yibin;Shu Xingtian CN111253249, 2020, A Location in patent:Paragraph 0090-0091
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