Benzenamine, 4-(2-propen-1-yl)- synthesis
- Product Name:Benzenamine, 4-(2-propen-1-yl)-
- CAS Number:32704-23-7
- Molecular formula:C9H11N
- Molecular Weight:133.19
Yield:-
Reaction Conditions:
with ammonium chloride in ethanol;water;
Steps:
86.B 4-allyl-phenylamine
Example 86B 4-allyl-phenylamine A solution of 1-allyl-4-nitro-benzene (1.92 g, 11.8 mmol), NH4Cl (1.89 g, 35.3 mmol) and iron powder (4.60 g, 82.4 mmol) in 3:1 ethanol:H2O (200 mL) was heated to reflux overnight. The reaction was cooled, concentrated under reduced pressure and purified on silica gel eluding with ethyl acetate to provide the titled compound. MS (ESI(+)) m/e 134 (M+H)+
References:
US2002/35137,2002,A1
53483-17-3
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